4-Methylbenzylamine → 4-(p-Tolylmethylamino)but-3-en-2-one
반응식
CO[CH:3]=[CH:4][C:5](=[O:7])[CH3:6].[CH3:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13][NH2:14])=[CH:11][CH:10]=1>>[C:9]1([CH3:8])[CH:16]=[CH:15][C:12]([CH2:13][NH:14][CH:3]=[CH:4][C:5](=[O:7])[CH3:6])=[CH:11][CH:10]=1참가 물질
3
실험 절차
The title compound 58 is prepared according to the procedure reported in step A of Example 18 with 4-methoxy-3-buten-2-one (0.103 g, 1 mmol) and 4-methylbenzylamine (0.125 g, 1 mmol) as reactants. Yellow oil. (Yield 0.19 g, 98%).
출처 및 근거
- ORD 기록
- ord-a8af7c49adf843baa0941499118aef4b
- 출처 데이터셋
- uspto-grants-2016_06
- 특허 번호
- US09376387B2
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