3-Bromopyridine-4-carboxaldehyde → HCID 118558022, 화합물

반응식

[CH3:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[C:7](=[O:11])[CH2:6][CH2:5]2.[Br:12][C:13]1[CH:14]=[N:15][CH:16]=[CH:17][C:18]=1[CH:19]=O>>[Br:12][C:13]1[CH:14]=[N:15][CH:16]=[CH:17][C:18]=1/[CH:19]=[C:6]1/[C:7](=[O:11])[C:8]2[C:4]([CH2:5]/1)=[CH:3][C:2]([CH3:1])=[CH:10][CH:9]=2

참가 물질

반응물 2

HCID 27629973-Bromopyridine-4-carboxaldehyde

HCID 101300315-Methyl-1-indanone

생성물 1

HCID 118558022HCID 118558022, 화합물

실험 절차

The title compound 90 is prepared according to the procedure reported in Example 34.1 with 5-methyl-1-indanone (0.73 g, 5 mmol) and 3-bromo-4-pyridinecarboxaldehyde (0.93 g, 5 mmol) as reactants. White solid. (Yield 1.24 g, 79%).

출처 및 근거

ORD 기록: ord-c411fc75233b4fb98182ca1aafaf0419
출처 데이터셋: uspto-grants-2016_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09376387B2

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