참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-Coumaric acid | HCID 322 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Glycidol | HCID 11164 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 용매 | Glycerol | HCID 753 | — |
| 생성물 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
반응 단계
17.4 g of p-hydroxy cinnamic acid and 40.0 g of glycidol were dissolved in 20 ml of DMSO, and catalytic amount of sulfuric acid was added. The solution was heated to 90° C. and then heating and agitation was carried out for 3 hours, neutralized by adding sodium hydroxide and then adduct of cinnamic acid and glycerin was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05426210 |
|---|
| 출처 데이터셋 | uspto-grants-1995_06 |
|---|
| ORD ID | ord-9fd1cb87e984445880ac895829b5f575 |
|---|
| 출처 메모 | uspto-grants-1995_06 |
|---|
