Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-Propenoic acid, 3-phenyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 4-Coumaric acid | HCID 322 | — |
| 반응물 | Nitrogen | HCID 947 | — |
| 반응물 | Glycidol | HCID 11164 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 용매 | Glycerol | HCID 753 | — |
| 생성물 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
반응 단계
8.719 g of p-hydroxy cinnamic acid was dissolved in 10 ml of DMSO, and 100 mg of sodium hydroxide was added. The mixture was stirred and heated to 90° C. under a flow of N2 gas. 19.7 g of glycidol was added gradually, heating and agitation was carried out for 2 hours, neutralized by adding hydrochloric acid and then the adduct of cinnamic acid and glycerin was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05426210 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-b76ea8f01bb84b6080b39c1bfb6ab1c0 |
| 출처 메모 | uspto-grants-1995_06 |