2-Bromo-1-(3,4-dimethoxyphenyl)ethan-1-one → HCID 117843230, 화합물

HRID 2209202노트

반응식

HRID 2209202 반응식
Br[CH2:2]C(C1C=CC(OC)=C(OC)C=1)=O.ClC1C=NNC=1C(OC)=O.[Cl:25][C:26]1[CH:27]=[N:28][N:29]([CH2:35][C:36]([C:38]2[CH:43]=[CH:42][C:41]([O:44][CH3:45])=[C:40]([O:46][CH3:47])[CH:39]=2)=[O:37])[C:30]=1[C:31]([O:33][CH3:34])=[O:32]>>[Cl:25][C:26]1[CH:27]=[N:28][N:29]([CH2:35][C:36]([C:38]2[CH:43]=[CH:42][C:41]([O:44][CH3:45])=[C:40]([O:46][CH3:47])[CH:39]=2)=[O:37])[C:30]=1[C:31]([O:33][CH2:34][CH3:2])=[O:32]

참가 물질

4

반응물 3

HCID 2704232-Bromo-1-(3,4-dimethoxyphenyl)ethan-1-oneHCID 7147513methyl 4-chloro-1H-pyrazole-3-carboxylateHCID 117843379HCID 117843379, 화합물

생성물 1

HCID 117843230HCID 117843230, 화합물

실험 절차

Following the procedure of Example 5.01, beginning with 2-bromo-1-(3,4-dimethoxyphenyl)ethanone (1.20 g, 4.63 mmol) and methyl 4-chloro-1H-pyrazole-5-carboxylate (855 mg, 5.33 mmol), methyl 4-chloro-1-(2-(3,4-dimethoxyphenyl)-2-oxoethyl)-1H-pyrazole-5-carboxylate 5.21 was synthesized.

후처리

  1. customwas synthesized

출처 및 근거

ORD 기록
ord-2b6c275804da4e60961d311bdeacafcd
출처 데이터셋
uspto-grants-2016_06
특허 번호
US09376441B2

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