참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-Coumaric acid | HCID 322 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
반응 단계
2.8 g of p-hydroxy cinnamic acid was dissolved in 3 ml of DMSO, and 10 mg of sodium hydride of which the oil was washed by hexane was added. The mixture was stirred and heated to 90° C. under a flow of N2 gas. 5.0 g of glycidol was added gradually, heating and agitation were carried out for 1.5 hours, neutralized by adding hydrochloric acid and then the adduct of cinnamic acid and glycerin was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05426210 |
|---|
| 출처 데이터셋 | uspto-grants-1995_06 |
|---|
| ORD ID | ord-2231e991bda54208932c1c846850f007 |
|---|
| 출처 메모 | uspto-grants-1995_06 |
|---|
