Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-Propenoic acid, 3-phenyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Glycidol | HCID 11164 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | Methyl isoferulate | HCID 6439893 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
반응 단계
3 g of methyl isoferulate was dissolved in 600 ml of DMSO, and 370 mg of sodium hydride was added. The system was heated to 90° C. under N2 gas flow and 7 g of glycidol was added gradually. Heating and agitation was carried out for 0.5 hours. The system was cooled, neutralized by adding hydrochloric acid, solvent was removed and adduct of cinnamic acid and glycerin was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05426210 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-f297ae3acb9542e7bf85a53dda6a37d2 |
| 출처 메모 | uspto-grants-1995_06 |