Thionyl Chloride → HCID 19035210, 화합물

HRID 2209987노트

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HRID 2209987 반응식
[F:1][C:2]1[C:10]([C:11]([F:14])([F:13])[F:12])=[C:9]([F:15])[CH:8]=[C:7]([F:16])[C:3]=1[C:4](O)=[O:5].S(Cl)([Cl:19])=O>>[F:1][C:2]1[C:10]([C:11]([F:14])([F:13])[F:12])=[C:9]([F:15])[CH:8]=[C:7]([F:16])[C:3]=1[C:4]([Cl:19])=[O:5]

참가 물질

3

반응물 2

HCID 24386Thionyl ChlorideHCID 27779962,4,6-Trifluoro-3-(trifluoromethyl)benzoic acid

생성물 1

HCID 19035210HCID 19035210, 화합물

반응 조건

온도
50 °C

실험 절차

5.8 g (0,024 mol) of 2,4,6-trifluoro-3-trifluoromethylbenzoic acid are added in portions at room temperature to 40 ml of thionyl chloride. After metering has ended, the mixture is heated at 50° C. until the evolution of gas has ceased. The excess thionyl chloride is then removed by distillation, and the crude product is reacted further directly.

후처리

  1. customThe excess thionyl chloride is then removed by distillation
  2. customthe crude product is reacted further directly

출처 및 근거

ORD 기록
ord-799914084c4b410cbd0f94c59343e7ce
출처 데이터셋
uspto-grants-1995_10
특허 번호
US05457104

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