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[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][C:6]([S:13]([OH:16])(=[O:15])=[O:14])=[CH:7][C:8]=2O)[C:3]=1[S:17]([OH:20])(=[O:19])=[O:18].FC1N=NN=C(F)C=1F.N1CCOCC1>>[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:8]([S:13]([OH:16])(=[O:15])=[O:14])=[CH:7][C:6]([S:13]([OH:16])(=[O:15])=[O:14])=[CH:5][C:4]=2[C:3]=1[S:17]([OH:20])(=[O:19])=[O:18]참가 물질
4
실험 절차
31.9 g of 2-amino-5-hydroxynaphthalene-1,7-disulphonic acid are condensed by the procedure of Example 1 with trifluorotriazine and then with morpholine. A diazo compound obtained in the usual manner by direct diazotisation of 38.3 g of 2-aminonaphthalene-1,5,7-trisulphonic acid is added to the resulting suspension of the monofluorotriazinyl compound at 5° to 10°, while simultaneously maintaining the pH at 7.0 to 7.5 by sprinkling in sodium bicarbonate. After coupling is complete, the dyestuff of the formula ##STR17## is salted out, filtered off with suction, dried and milled.
출처 및 근거
- ORD 기록
- ord-130abafe0e2e4a3c96cefd5c49c5de34
- 출처 데이터셋
- uspto-grants-1995_10
- 특허 번호
- US05459245
연결된 노트
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