4-Chlorobenzenesulfonyl chloride → 1-(2-(p-Chlorobenzenesulphonylamino)ethyl)naphthalene

HRID 22107

반응식

HRID 22107 반응식
[NH2:1][CH2:2][CH2:3][C:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[CH:7]=[CH:6][CH:5]=1.[Cl:14][C:15]1[CH:20]=[CH:19][C:18]([S:21](Cl)(=[O:23])=[O:22])=[CH:17][CH:16]=1>>[Cl:14][C:15]1[CH:20]=[CH:19][C:18]([S:21]([NH:1][CH2:2][CH2:3][C:4]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[CH:7]=[CH:6][CH:5]=2)(=[O:23])=[O:22])=[CH:17][CH:16]=1

참가 물질

3

반응물 2

HCID 73984-Chlorobenzenesulfonyl chlorideHCID 208531-Naphthaleneethanamine

생성물 1

HCID 150570151-(2-(p-Chlorobenzenesulphonylamino)ethyl)naphthalene

실험 절차

Prepared from 1-(2-aminoethyl)naphthalene and 4-chlorobenzenesulphonic acid chloride analogously to Example 1a. The crude product was purified by column chromatography on silica gel using ethylene chloride/cyclohexane (2:1).

후처리

  1. customThe crude product was purified by column chromatography on silica gel

출처 및 근거

ORD 기록
ord-63effced1d994800bc9aeab5fb8189b3
출처 데이터셋
uspto-grants-1995_06
특허 번호
US05426119

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