Thionyl Chloride → HCID 88422751, 화합물

반응식

[CH3:1][C:2]1[CH:3]=[C:4]([CH:11]=[C:12]([CH3:14])[CH:13]=1)[CH2:5][CH:6]([OH:10])[C:7](O)=[O:8].S(Cl)([Cl:17])=O>>[CH3:1][C:2]1[CH:3]=[C:4]([CH:11]=[C:12]([CH3:14])[CH:13]=1)[CH2:5][CH:6]([OH:10])[C:7]([Cl:17])=[O:8]

참가 물질

반응물 2

HCID 24386Thionyl Chloride

HCID 19379351HCID 19379351, 화합물

생성물 1

HCID 88422751HCID 88422751, 화합물

실험 절차

3,5-Dimethyl benzyl glycolic acid (5.59 g) was cooled to 0° C. Thionyl chloride (5 ml) was added and the stirred solution was refluxed for 2 h. The solvent was removed in vacuo to afford 3,5-dimethyl benzyl glycolic acid chloride as an oil.

후처리

temperaturethe stirred solution was refluxed for 2 h
customThe solvent was removed in vacuo

출처 및 근거

ORD 기록: ord-dd92091af385400ca76de8145c5d9c4b
출처 데이터셋: uspto-grants-1995_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05459270

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