Methyl isothiocyanate → HCID 14518105, 화합물

HRID 2210806노트

반응식

HRID 2210806 반응식
[CH3:1][O:2][CH:3]([O:6][CH3:7])[CH2:4][NH2:5].[N:8]([CH3:11])=[C:9]=[S:10]>O1CCCC1>[CH3:1][O:2][CH:3]([O:6][CH3:7])[CH2:4][NH:5][C:9]([NH:8][CH3:11])=[S:10]

참가 물질

4

반응물 2

HCID 11167Methyl isothiocyanateHCID 89728Aminoacetaldehyde dimethyl acetal

생성물 1

HCID 14518105HCID 14518105, 화합물수율 99.7%

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

A mixture of 4.2 g of 2,2-dimethoxyethanamine, 3.6 g of isothiocyanatomethane and 100 ml of tetrahydrofuran was stirred overnight. The reaction mixture was evaporated, yielding 7.1 g (99%) of N-(2,2-dimethoxyethyl)-N'-methylthiourea as an oily residue (interm. 34);

후처리

  1. customThe reaction mixture was evaporated

출처 및 근거

ORD 기록
ord-9bfb0dcacdfc4b46bd67dd709ee3b9d7
출처 데이터셋
uspto-grants-1995_10
특허 번호
US05461050

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