3-Phenylpropyl 4-methylbenzenesulfonate → 4-Phenylbutyl 4-methylbenzenesulfonate

HRID 2211074

반응식

HRID 2211074 반응식
[CH2:1]([CH:11]1[CH2:19][C:18]2[C:13](=[CH:14][CH:15]=[C:16](C3N=CC(O)=CN=3)[CH:17]=2)C1)[CH2:2]CCCCCCCC.C(C1C=CC(C2SC(C3C=CC(O)=CC=3)=CN=2)=CC=1)CCCCC.[C:51]1([CH3:70])[CH:56]=[CH:55][C:54]([S:57]([O:60]CCCC2C=CC=CC=2)(=[O:59])=[O:58])=[CH:53][CH:52]=1>>[C:51]1([CH3:70])[CH:52]=[CH:53][C:54]([S:57]([O:60][CH2:2][CH2:1][CH2:11][CH2:19][C:18]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)(=[O:58])=[O:59])=[CH:55][CH:56]=1

참가 물질

4

반응물 3

HCID 109899213-Phenylpropyl 4-methylbenzenesulfonateHCID 193753532-(2-Decylindan-5-yl)pyrimidine-5-olHCID 233547624-{2-(4-Hexylphenyl)thiazole-5-yl}phenol

생성물 1

HCID 152128864-Phenylbutyl 4-methylbenzenesulfonate수율 71.1%

실험 절차

An objective product was prepared in the same manner as in Example 2 except that 2-(2-decylindan-5-yl)pyrimidine-5-ol was changed to 4-{2-(4-hexylphenyl)thiazole-5-yl}phenol and 3-phenylpropyl p-toluenesulfonate was changed to 4-phenylbutyl p-toluenesulfonate (Yield: 71.1%).

출처 및 근거

ORD 기록
ord-00c4901eedf9453b9195bf79579ab36a
출처 데이터셋
uspto-grants-1995_10
특허 번호
US05462694

연결된 노트

불러오는 중…