Potassium Iodide → 3-Iodopentafluoropropene-1
반응식
[I-:1].[K+].S(F)(O[C:7]([F:14])([F:13])[C:8]([F:12])=[C:9]([F:11])[F:10])(=O)=O>COCCOCCOCCOCCOC>[F:13][C:7]([I:1])([F:14])[C:8]([F:12])=[C:9]([F:11])[F:10]참가 물질
4
반응 조건
- 온도
- 20 °C
실험 절차
Perfluoroallyl iodide (CF2CFCF2I) was prepared by transferring 8.5 g of dry potassium iodide, 20 ml of tetraglyme and 42.5 millimoles of perfluoroallyl fluorosulfate by vacuum line to a 100-ml flask. The mixture was warmed to 20° C. and stirred for 12 hours in a dark room. The mixture was then fractionated through -100° C. and -196° C. traps, with the product being collected in the -100° C. trap.
후처리
- customwas then fractionated through -100° C. and -196° C.
- customwith the product being collected in the -100° C. trap
출처 및 근거
- ORD 기록
- ord-5394dfafca674a508bd928d8ebb1c478
- 출처 데이터셋
- uspto-grants-1995_10
- 특허 번호
- US05463005
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