참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1,5-Dimethoxy-2,4-dinitrobenzene | HCID 615053 | — |
| 용매 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 생성물 | 4,6-Dinitroresorcinol | HCID 61158 | 95% |
반응 단계
A 100 mL, 3-necked, round-bottom flask is charged with 30 mL of N-methylpyrrolidinone, 2.6 g (0.02 mole) of 1,3-dimethoxy-4,6-dinitrobenzene. The resulting solution is heated to 130° C. for two to three hours. The reaction mixture is then cooled and poured into an excess of dilute hydrochloric acid. The resulting solid is isolated by filtration to yield 1.9 g (95% yield) of 4,6-dinitroresorcinol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05463129 |
|---|
| 출처 데이터셋 | uspto-grants-1995_10 |
|---|
| ORD ID | ord-ee69f858690d47bab1c6767ca626beb8 |
|---|
| 출처 메모 | uspto-grants-1995_10 |
|---|
