Allyl bromide → Methyl 4-{3-[(prop-2-en-1-yl)oxy]phenoxy}benzoate

반응식

[OH:1][C:2]1[CH:3]=[C:4]([CH:16]=[CH:17][CH:18]=1)[O:5][C:6]1[CH:15]=[CH:14][C:9]([C:10]([O:12][CH3:13])=[O:11])=[CH:8][CH:7]=1.[CH2:19](Br)[CH:20]=[CH2:21]>>[CH2:21]([O:1][C:2]1[CH:3]=[C:4]([CH:16]=[CH:17][CH:18]=1)[O:5][C:6]1[CH:15]=[CH:14][C:9]([C:10]([O:12][CH3:13])=[O:11])=[CH:8][CH:7]=1)[CH:20]=[CH2:19]

참가 물질

반응물 2

HCID 7841Allyl bromide

HCID 19375802HCID 19375802, 화합물

생성물 1

HCID 19375796Methyl 4-{3-[(prop-2-en-1-yl)oxy]phenoxy}benzoate수율 96%

실험 절차

The title compound was prepared in 96% yield as an oil from methyl 4-(3-hydroxyphenoxy)benzoate and allyl bromide by the procedure of Preparation 36. NMR.

출처 및 근거

ORD 기록: ord-c9f3fe53b264401f973d8f69b6f0c652
출처 데이터셋: uspto-grants-1995_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05462954

반응 노트

불러오는 중…