Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(4-hydroxy-2,3,6-trimethylphenyl)formamide → N-[4-[[(E)-3-(4-Isopropylphenyl)-2-propenyl]oxy]-2,3,6-trimethylphenyl]formamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(4-hydroxy-2,3,6-trimethylphenyl)formamide | HCID 21961295 | — |
| 반응물 | 1-[(E)-3-bromo-1-propenyl]-4-isopropylbenzene | HCID 21961313 | — |
| 용매 | Ethyl acetate hexane | HCID 21226206 | — |
| 생성물 | N-[4-[[(E)-3-(4-Isopropylphenyl)-2-propenyl]oxy]-2,3,6-trimethylphenyl]formamide | HCID 21961342 | 59% |
반응 단계
By using N-(4-hydroxy-2,3,6-trimethylphenyl)formamide and 1-[(E)-3-bromo-1-propenyl]-4-isopropylbenzene, the title compound was synthesized according to Reference Example 17a. Yield: 59%. Melting point: 165-167° C. (Ethyl acetate-hexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07101867B2 |
| 출처 데이터셋 | uspto-grants-2006_09 |
| ORD ID | ord-495416fcdabc447c842a415e4c44d07f |
| 출처 메모 | uspto-grants-2006_09 |