Water → Cyclopropanesulphonylbenzene

HRID 2212062노트

반응식

HRID 2212062 반응식
[C:1]1([S:7][CH:8]2[CH2:10][CH2:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH:11]OS([O-])=O.[K+].[OH2:17]>CO>[CH:8]1([S:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)(=[O:11])=[O:17])[CH2:10][CH2:9]1

참가 물질

5

반응물 3

HCID 962WaterHCID 123348Cyclopropyl phenyl sulfideHCID 23707502Potassium hydroxy sulfite

생성물 1

HCID 11309899Cyclopropanesulphonylbenzene

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

A solution of cyclopropyl phenyl sulfide (10.5 g, 70 mmol) and Oxone™ (55.13 g, 175 mmol) in methanol (30 ml) was stirred at room temperature for 5 hours. The mixture was diluted was water and extracted with ethyl acetate. The combined organic layers were dried (MgSO4) and concentrated in vacuo.

후처리

  1. additionThe mixture was diluted
  2. extractionextracted with ethyl acetate
  3. dry with materialThe combined organic layers were dried (MgSO4)
  4. concentrationconcentrated in vacuo

출처 및 근거

ORD 기록
ord-cf85ed6b24364e7f880c4edaa04925ef
출처 데이터셋
uspto-grants-2006_09
특허 번호
US07101892B2

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