Methanol → HCID 59896206, 화합물

반응식

[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([OH:10])=[O:9])[NH2:7].[CH3:11]O>>[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([O:10][CH3:11])=[O:9])[NH2:7]

참가 물질

반응물 2

HCID 887Methanol

HCID 99558S-(2-Aminoethyl)-L-cysteine

생성물 1

HCID 59896206HCID 59896206, 화합물

실험 절차

A 10 g (50 mmol) sample of S-(2-aminoethyl)-L-cysteine was dissolved in 400 mL of methanol. Into this cooled solution was bubbled in anhydrous HCl for 30 minutes. After stirring at room temperature overnight, the solution was concentrated to afford 12.7 g of the title compound.

후처리

customInto this cooled solution was bubbled in anhydrous HCl for 30 minutes
concentrationthe solution was concentrated

출처 및 근거

ORD 기록: ord-6d845bb2135b4f2eb5c19437b15f5d94
출처 데이터셋: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07102013B2

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