Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → tert-Butyl ((1H-benzo[d]imidazol-2-yl)methyl)carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 1,2-Phenylenediamine dihydrochloride | HCID 11990 | — |
| 반응물 | tert-butyl N-(cyanomethyl)carbamate | HCID 545844 | — |
| 반응물 | HCID 178418582 | HCID 178418582 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | tert-Butyl ((1H-benzo[d]imidazol-2-yl)methyl)carbamate | HCID 11448004 | — |
반응 단계
3.32 g of a 30% NaOCH3 solution were added to tert-butyl cyanomethylcarbamate (3 g; 19.21 mmol) in 20 ml of CH3OH, and the mixture was stirred at room temperature for 1 h. After addition of 3.4 g of 1,2-phenylenediamine bishydrochloride, the reaction mixture was stirred further overnight and then added to 100 ml of H2O, and the resulting solid was filtered off and dried in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07105508B1 |
| 출처 데이터셋 | uspto-grants-2006_09 |
| ORD ID | ord-dbbdafbfa47c4854b58d80974b580e8b |
| 출처 메모 | uspto-grants-2006_09 |