4-(Dimethylamino)Benzaldehyde → (4-Butylphenyl)[(4-dimethylaminophenyl)methyl]amine

반응식

[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH2:12]([C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1)[CH2:13][CH2:14][CH3:15]>>[CH2:12]([C:16]1[CH:17]=[CH:18][C:19]([NH:20][CH2:7][C:6]2[CH:9]=[CH:10][C:3]([N:2]([CH3:11])[CH3:1])=[CH:4][CH:5]=2)=[CH:21][CH:22]=1)[CH2:13][CH2:14][CH3:15]

참가 물질

반응물 2

HCID 74794-(Dimethylamino)Benzaldehyde

HCID 76944-Butylaniline

생성물 1

HCID 21957943(4-Butylphenyl)[(4-dimethylaminophenyl)methyl]amine수율 36.1%

실험 절차

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (10.0 g) and 4-butylaniline (10.0 g) as starting materials, (4-butylphenyl)[(4-dimethylaminophenyl)methyl]amine (6.83 g) was obtained. melting point: 60–61° C.

후처리

customBy the reaction and treatment in the same manner

출처 및 근거

ORD 기록: ord-20df0cbc23c54e46a56e537a7fdc4b44
출처 데이터셋: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07105567B2

반응 노트

불러오는 중…