4-(Dimethylamino)Benzaldehyde → [(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amine

HRID 2213585

반응식

HRID 2213585 반응식
[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH2:12]([C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][CH:15]=1)[CH3:13]>>[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:18][C:17]2[CH:19]=[CH:20][C:14]([CH2:12][CH3:13])=[CH:15][CH:16]=2)=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 74794-(Dimethylamino)BenzaldehydeHCID 115044-Ethylaniline

생성물 1

HCID 3482181[(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amine수율 62.8%

실험 절차

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (10 g) and 4-ethylaniline (8.12 g) as starting materials, [(4-dimethylaminophenyl)methyl](4-ethylphenyl)amine (10.7 g) was obtained. melting point: 64–66° C.

후처리

  1. customBy the reaction and treatment in the same manner

출처 및 근거

ORD 기록
ord-109b14d068bf435b9db2073fdb5eff4b
출처 데이터셋
uspto-grants-2006_09
특허 번호
US07105567B2

연결된 노트

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