4-(Dimethylamino)Benzaldehyde → [(4-Dimethylaminophenyl)methyl](4-propylphenyl)amine

반응식

[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH2:12]([C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1)[CH2:13][CH3:14]>>[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:19][C:18]2[CH:20]=[CH:21][C:15]([CH2:12][CH2:13][CH3:14])=[CH:16][CH:17]=2)=[CH:5][CH:4]=1

참가 물질

반응물 2

HCID 74794-(Dimethylamino)Benzaldehyde

HCID 759084-Propylaniline

생성물 1

HCID 21957946[(4-Dimethylaminophenyl)methyl](4-propylphenyl)amine수율 88.9%

실험 절차

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (11 g) and 4-propylaniline (10 g) as starting materials, [(4-dimethylaminophenyl)methyl](4-propylphenyl)amine (17.6 g) was obtained. melting point: 74–76° C.

후처리

customBy the reaction and treatment in the same manner

출처 및 근거

ORD 기록: ord-ec6491252ae0416a9b7096bcc365fb10
출처 데이터셋: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07105567B2

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