Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzonitrile → 1-Phenyl-1-hexyne
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzonitrile | HCID 7505 | — |
| 반응물 | Phenylacetylene | HCID 10821 | — |
| 반응물 | 1-Hexyne | HCID 12732 | — |
| 생성물 | 1-Phenyl-1-hexyne | HCID 136908 | 95% |
반응 단계
The procedure was identical to Example 1, with the exception that 1-hexyne (0.450 ml; 0.329 g; 4.00 mmol) was used as a substrate instead of phenylacetylene. GC analysis of the organic phase of the hydrolyzed reaction sample after 20 h at 65° C. showed the presence of 1.90 mmol (95% yield) of 1-hexynylbenzene and and 0.08 mmol of benzonitrile remaining in the reaction mixture.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07105707B2 |
| 출처 데이터셋 | uspto-grants-2006_09 |
| ORD ID | ord-585442bfbe2140c0afdecb052599d445 |
| 출처 메모 | uspto-grants-2006_09 |