Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzonitrile → Benzene, 1-methyl-4-(phenylethynyl)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzonitrile | HCID 7505 | — |
| 반응물 | Phenylacetylene | HCID 10821 | — |
| 반응물 | p-Ethynyltoluene | HCID 13018 | — |
| 생성물 | Benzene, 1-methyl-4-(phenylethynyl)- | HCID 3014187 | 81% |
반응 단계
The procedure was identical to Example 1, with the exception that 4-ethynyltoluene (0.507 ml; 0.465 g; 4.00 mmol) was used as a substrate instead of phenylacetylene. GC analysis of the organic phase of the hydrolyzed reaction sample after 42 h at 65° C. showed the presence of 1.62 mmol (81% yield) of 1-methyl-4-(phenylethynyl)benzene, and 0.25 mmol of benzonitrile remaining in the reaction mixture.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07105707B2 |
| 출처 데이터셋 | uspto-grants-2006_09 |
| ORD ID | ord-6ef020ade22348b8a18215c8077c6abe |
| 출처 메모 | uspto-grants-2006_09 |