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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2213976생성일: 2026년 10월 26일

Benzonitrile → Benzene, 1-methyl-4-(phenylethynyl)-

https://huagongshe.com/reaction/2213976

반응식

참여 물질

역할이름HCID투입량
반응물BenzonitrileHCID 7505—
반응물PhenylacetyleneHCID 10821—
반응물p-EthynyltolueneHCID 13018—
생성물Benzene, 1-methyl-4-(phenylethynyl)-HCID 301418781%

반응 단계

The procedure was identical to Example 1, with the exception that 4-ethynyltoluene (0.507 ml; 0.465 g; 4.00 mmol) was used as a substrate instead of phenylacetylene. GC analysis of the organic phase of the hydrolyzed reaction sample after 42 h at 65° C. showed the presence of 1.62 mmol (81% yield) of 1-methyl-4-(phenylethynyl)benzene, and 0.25 mmol of benzonitrile remaining in the reaction mixture.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07105707B2
출처 데이터셋uspto-grants-2006_09
ORD IDord-6ef020ade22348b8a18215c8077c6abe
출처 메모uspto-grants-2006_09