Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
m-Nitroacetophenone → 2-Bromo-1-(3-nitrophenyl)ethan-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | m-Nitroacetophenone | HCID 8494 | — |
| 반응물 | Pyridiniumtribromide | HCID 21124087 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 2-Bromo-1-(3-nitrophenyl)ethan-1-one | HCID 75213 | 127.1% |
반응 단계
m-Nitroacetophenone (20 g) was dissolved in acetic acid (150 mL) under argon. Pyridinium tribromide (38.7 g) was added at once; the reaction was allowed to stir at room temperature for 1 hour and then quenched with water (250 mL). The product was filtered and air dried to give the title compound (25 g, 84%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08207167B2 |
| 출처 데이터셋 | uspto-grants-2012_06 |
| ORD ID | ord-c14ea3eb512c47819ba451df036c0cd2 |
| 출처 메모 | uspto-grants-2012_06 |