홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Hydrazine → HCID 21947598, 화합물

HRID 2214432
노트
인쇄 미리보기

반응식

HRID 2214432 반응식
[CH3:1][C:2]1[N:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][N:12]2C(=O)C3C(=CC=CC=3)C2=O)=[CH:4][CH:3]=1.NN>C(O)C>[CH3:1][C:2]1[N:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][NH2:12])=[CH:4][CH:3]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 21947595HCID 21947595, 화합물

생성물 1

HCID 21947598HCID 21947598, 화합물수율 116.8%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A mixture of 2-4 (7.2 g, 24.5 mmol), hydrazine (3.8 mL), and ethanol (500 mL) was heated at reflux for 4 hours. The resulting mixture was cooled and filtered, and the filtrate concentrated to give 2-5 as a yellow solid (4.7 g) contaminated with some phthalhydrazide.

후처리

  1. temperaturewas heated
  2. temperatureat reflux for 4 hours
  3. temperatureThe resulting mixture was cooled
  4. filtrationfiltered
  5. concentrationthe filtrate concentrated

출처 및 근거

ORD 기록
ord-0f76b292b1834ee9a3cb1ea97addaf33
출처 데이터셋
uspto-grants-2006_09
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07109191B2

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트