1-[Benzyl(methyl)amino]-3-hexanone → 1-(Benzyl-methyl-amino)-hexan-3-ol

HRID 2218085

반응식

HRID 2218085 반응식
[CH2:1]([N:8]([CH3:17])[CH2:9][CH2:10][CH:11]([OH:16])[CH2:12][CH2:13][CH2:14]C)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(N(C)CCC(=O)CCC)C1C=CC=CC=1>>[CH2:1]([N:8]([CH3:17])[CH2:9][CH2:10][CH:11]([OH:16])[CH2:12][CH2:13][CH3:14])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 4195861-[Benzyl(methyl)amino]-3-hexanoneHCID 179819331-(Benzyl-methyl-amino)-heptan-3-ol

생성물 1

HCID 179819281-(Benzyl-methyl-amino)-hexan-3-ol

실험 절차

Using a method similar to that for 1-(Benzyl-methyl-amino)-heptan-3-ol, 1-(benzyl-methyl-amino)-hexan-3-one affords the title compound: mass spectrum (ion spray) m/z 222 (M+1); 1H NMR (CDCl3) δ 7.34-7.24 (m, 5H), 3.79-3.73 (m, 1H), 3.55 (dd, 2H), 2.81-2.74 (m, 1H), 2.59-2.55 (m, 1H), 2.22 (s, 3H), 1.72-1.62 (m, 1H), 1.56-1.31 (m, 5H), 0.93 (t, 3H).

출처 및 근거

ORD 기록
ord-ce2a152a10ee4e05a3cac1a39510b8b2
출처 데이터셋
uspto-grants-2008_08
특허 번호
US07410982B2

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