4-Hydrazinobenzonitrile → 4-(5-Amino-3-tert-butyl-1H-pyrazol-1-yl)benzonitrile

HRID 221859

반응식

HRID 221859 반응식
[C:1]([C:5]1[CH:6]=[C:7]([NH2:19])[N:8]([C:10]2[CH:15]=[CH:14][C:13]([N+]([O-])=O)=[CH:12][CH:11]=2)[N:9]=1)([CH3:4])([CH3:3])[CH3:2].[C:20](C1C=CC(NN)=CC=1)#[N:21]>>[NH2:19][C:7]1[N:8]([C:10]2[CH:15]=[CH:14][C:13]([C:20]#[N:21])=[CH:12][CH:11]=2)[N:9]=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH:6]=1

참가 물질

3

반응물 2

HCID 5837844-HydrazinobenzonitrileHCID 13023603-tert-butyl-1-(4-nitrophenyl)-1H-pyrazol-5-amine

생성물 1

HCID 71470834-(5-Amino-3-tert-butyl-1H-pyrazol-1-yl)benzonitrile수율 85%

실험 절차

The title compound was prepared (85% yield) in the same manner as described for 5-tert-butyl-2-(4-nitro-phenyl)-2H-pyrazol-3-ylamine, replacing 4-nitrophenylhydrazine with 4-cyanophenylhydrazine. MS LC-MS [M+H]+=241, RT=2.39 min.

출처 및 근거

ORD 기록
ord-3df769860f44417bb3f955adb3f7aa03
출처 데이터셋
uspto-grants-2012_06
특허 번호
US08207166B2

연결된 노트

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