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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2220042생성일: 2026년 10월 27일

Lauryl acrylate → Behenyl methacrylate lauryl acrylate vinyl acetate

https://huagongshe.com/reaction/2220042

반응식

참여 물질

역할이름HCID투입량
반응물Lauryl acrylateHCID 75084—
반응물2-Propenoic acid, 2-methyl-, docosyl esterHCID 3034258—
용매O-XyleneHCID 7237—
생성물Behenyl methacrylate lauryl acrylate vinyl acetateHCID 86600777—

반응 조건

온도60 °C

반응 단계

Xylene (15 g), behenyl methacrylate (15 g), lauryl acrylate (2 g), are charged to a reactor equipped with a stirrer, a heater, a thermometer, and a nitrogen-bubbling duct. The reactor is flushed with nitrogen gas and sealed. Then vinyl acetate (2 g) is charged. The reactor is heated to 60° C. and 2,2′-azobis(2-methyl, ethyl-propionitrile) (0.06 g) is added. The reaction mixture is heated in the closed system at 75° C. for one hour, at 90° C. for 30 minutes, and at 110° C. for one hour to provide behenyl methacrylate/lauryl acrylate/vinyl acetate polymer having a number average molecular weight of 41,008 Daltons with polydispersity 3.4. The viscosity of the polymer is 135 cP at 20° C. as a 40% solution in toluene.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07417009B2
출처 데이터셋uspto-grants-2008_08
ORD IDord-c00d7738bf3c4d6d80c6043342f5c143
출처 메모uspto-grants-2008_08