참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Lauryl acrylate | HCID 75084 | — |
| 반응물 | 2-Propenoic acid, 2-methyl-, docosyl ester | HCID 3034258 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | Behenyl methacrylate lauryl acrylate vinyl acetate | HCID 86600777 | — |
반응 단계
Xylene (15 g), behenyl methacrylate (15 g), lauryl acrylate (2 g), are charged to a reactor equipped with a stirrer, a heater, a thermometer, and a nitrogen-bubbling duct. The reactor is flushed with nitrogen gas and sealed. Then vinyl acetate (2 g) is charged. The reactor is heated to 60° C. and 2,2′-azobis(2-methyl, ethyl-propionitrile) (0.06 g) is added. The reaction mixture is heated in the closed system at 75° C. for one hour, at 90° C. for 30 minutes, and at 110° C. for one hour to provide behenyl methacrylate/lauryl acrylate/vinyl acetate polymer having a number average molecular weight of 41,008 Daltons with polydispersity 3.4. The viscosity of the polymer is 135 cP at 20° C. as a 40% solution in toluene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07417009B2 |
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| 출처 데이터셋 | uspto-grants-2008_08 |
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| ORD ID | ord-c00d7738bf3c4d6d80c6043342f5c143 |
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| 출처 메모 | uspto-grants-2008_08 |
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