Diethylamine → (2-Bromo-benzyl)-diethyl-amine
반응식
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8]Br.[CH2:10]([NH:12][CH2:13][CH3:14])[CH3:11]>C1(C)C=CC=CC=1>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][N:12]([CH2:13][CH3:14])[CH2:10][CH3:11]참가 물질
4
실험 절차
To 1-Bromo-2-bromomethyl-benzene (2.17 g, 0.008 mmol) in toluene (15 mL) was added diethylamine (3.05 mL) and the mixture was stirred at room temperature for 14 hours. The reaction mixture was filtered and concentrated to give Example 229A as an oil.
후처리
- filtrationThe reaction mixture was filtered
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-ca758fde160a49c097dfedcef981117c
- 출처 데이터셋
- uspto-grants-2008_08
- 특허 번호
- US07417040B2
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