Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(Benzyl-methyl-amino)-heptan-3-one → 1-[Benzyl(methyl)amino]-3-hexanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(Benzyl-methyl-amino)-heptan-3-one | HCID 17981922 | — |
| 반응물 | HCID 178455855 | HCID 178455855 | — |
| 생성물 | 1-[Benzyl(methyl)amino]-3-hexanone | HCID 419586 | — |
반응 단계
Using a method similar to that for 1-(Benzyl-methyl-amino)-heptan-3-one, propylmagnesium chloride (2 M solution in diethyl ether) affords the title compound: mass spectrum (ion spray) m/z=220 (M+1): 1H NMR (CDCl3) δ 7.35-7.24 (m, 5H), 3.51 (s, 2H), 2.74-2.69 (m, 2H), 2.66-2.61 (m, 2H), 2.39 (t, 2H), 2.20 (s, 3H), 1.67-1.57 (m, 2H), 0.92(t, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07417064B2 |
| 출처 데이터셋 | uspto-grants-2008_08 |
| ORD ID | ord-5981ee199ffe46258ddf07838c48ee81 |
| 출처 메모 | uspto-grants-2008_08 |