Dipentylamine → HCID 178446345, 화합물

HRID 2222081

반응식

HRID 2222081 반응식
[I-:1].[I-].[I-].[CH2:4]([N:7]([C:11]1[CH:12]=[CH:13][C:14]2[C:23]([CH:24]=1)=[S+:22][C:21]1[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=1)[N:15]=2)[CH2:8][CH2:9][CH3:10])[CH2:5][CH3:6].C(N([C:32]1[CH:33]=[CH:34][C:35]2C([CH:45]=1)=[S+]C1[C:37](=[CH:38][CH:39]=[CH:40][CH:41]=1)[N:36]=2)CCC)CC.C(N(C1C=CC2C(C=1)=[S+]C1C(=CC=CC=1)N=2)CCC)CC.C(NCCCCC)CCCC>>[I-:1].[CH2:37]([N:36]([C:19]1[CH:18]=[CH:17][C:16]2[C:21]([CH:20]=1)=[S+:22][C:23]1[C:14](=[CH:13][CH:12]=[C:11]([N:7]([CH2:8][CH2:9][CH3:10])[CH2:4][CH2:5][CH3:6])[CH:24]=1)[N:15]=2)[CH2:35][CH2:34][CH2:33][CH2:32][CH3:45])[CH2:38][CH2:39][CH2:40][CH3:41]

참가 물질

3

반응물 2

HCID 16316DipentylamineHCID 178457153HCID 178457153, 화합물

생성물 1

HCID 178446345HCID 178446345, 화합물

실험 절차

This compound was obtained following isolation of 3-(N,N-dipropylamino)-phenothiazin-5-ium triiodide and subsequent treatment with dipentylamine. Precipitation from dichloromethane by addition of diethyl ether yielded purple lustrous crystals. Mass spectrometry: C28H42N3OS requires m/z=452; found m/z=452 (I− not detected by mass spectrometry).

후처리

  1. customThis compound was obtained
  2. customPrecipitation from dichloromethane
  3. additionby addition of diethyl ether yielded purple lustrous crystals

출처 및 근거

ORD 기록
ord-5235de8511c244119ac2aa6d8ed2459b
출처 데이터셋
uspto-grants-2008_05
특허 번호
US07371744B2

연결된 노트

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