3,4-Dimethoxybenzeneacetonitrile → HCID 10405853, 화합물

반응식

[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][C:7]([CH:8]=O)=[CH:6][C:5]=1[N+:12]([O-:14])=[O:13])[CH3:2].[CH3:15][O:16][C:17]1[CH:18]=[C:19]([CH:23]=[CH:24][C:25]=1[O:26][CH3:27])[CH2:20][C:21]#[N:22]>>[CH3:15][O:16][C:17]1[CH:18]=[C:19](/[C:20](=[CH:8]/[C:7]2[CH:10]=[CH:11][C:4]([O:3][CH2:1][CH3:2])=[C:5]([N+:12]([O-:14])=[O:13])[CH:6]=2)/[C:21]#[N:22])[CH:23]=[CH:24][C:25]=1[O:26][CH3:27]

참가 물질

반응물 2

HCID 667273,4-Dimethoxybenzeneacetonitrile

HCID 14943794-Ethoxy-3-nitrobenzaldehyde

생성물 1

HCID 10405853HCID 10405853, 화합물수율 40%

실험 절차

4-Ethoxy-3-nitrobenzaldehyde (586 mg) and 3,4-dimethoxybenzyl cyanide (532 mg) were subjected to condensation in accordance with process B of (production process 2), to thereby produce the target product (425 mg, yield: 40%).

출처 및 근거

ORD 기록: ord-3e071da0e39549c5827f29421e788d7f
출처 데이터셋: uspto-grants-2008_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07371773B2

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