Benzyl 2-amino-2-methylpropanoate hydrochloride → Benzyl 2-amino-2-methylpropanoate
반응식
Cl.[NH2:2][C:3]([CH3:15])([CH3:14])[C:4]([O:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:5]>C(OCC)(=O)C>[NH2:2][C:3]([CH3:15])([CH3:14])[C:4]([O:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:5]참가 물질
3
실험 절차
Benzyl 2-amino-2-methylpropionate hydrochloride (1.48 g) was dissolved in ethyl acetate (60 mL) and a saturated aqueous sodium hydrogen carbonate solution (20 mL), and the organic layer was separated. The organic layer was washed with brine, and dried over anhydrous magnesium sulfate. The solvent was removed under reduced pressure to give the title compound (1.2 g).
후처리
- customa saturated aqueous sodium hydrogen carbonate solution (20 mL), and the organic layer was separated
- washThe organic layer was washed with brine
- dry with materialdried over anhydrous magnesium sulfate
- customThe solvent was removed under reduced pressure
출처 및 근거
- ORD 기록
- ord-c2d94bb84f8d4e2e9fb78401bd10114c
- 출처 데이터셋
- uspto-grants-2008_05
- 특허 번호
- US07375087B2
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