1,3-Dichloro-2-propanol → 2-Propanol, 1,3-bis[(2-hydroxyethyl)phenylamino]-
반응식
[OH:1][CH2:2][CH2:3][NH:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[C:11](=[O:14])([O-])[O-].[Ca+2].Cl[CH2:17][CH:18]([OH:21])[CH2:19]Cl>O>[OH:1][CH2:2][CH2:3][N:4]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)[CH2:17][CH:18]([OH:21])[CH2:19][N:4]([CH2:3][CH2:11][OH:14])[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1참가 물질
5
실험 절차
The mixture consisting of 2 moles (274.4 g) of N-β-hydroxyethylaniline, 140 g of calcium carbonate and 1.2 moles (154.8 g) of 1,3-dichloro-2-propanol in 1 liter of water is heated for 6 hours under water reflux.
후처리
- temperatureis heated for 6 hours under water
- temperaturereflux
출처 및 근거
- ORD 기록
- ord-0f296d5c90c541ba8c1f1c4edeaf06ee
- 출처 데이터셋
- uspto-grants-1994_09
- 특허 번호
- US05344464
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