3-Buten-1-ol → HCID 11358365, 화합물

HRID 2228342

반응식

HRID 2228342 반응식
[CH3:1][Si:2]([CH3:12])([CH3:11])[O:3][SiH:4]([CH3:10])[O:5][Si:6]([CH3:9])([CH3:8])[CH3:7].[CH2:13]([OH:17])[CH2:14][CH:15]=[CH2:16]>>[CH3:10][Si:4]([CH2:16][CH2:15][CH2:14][CH2:13][OH:17])([O:5][Si:6]([CH3:9])([CH3:8])[CH3:7])[O:3][Si:2]([CH3:11])([CH3:12])[CH3:1]

참가 물질

3

반응물 2

HCID 693893-Buten-1-olHCID 74640Trimethyl-[methyl(trimethylsilyloxy)silyl]oxysilane

생성물 1

HCID 11358365HCID 11358365, 화합물수율 83%

실험 절차

The reaction of Example 2a was repeated using 1,1,1,3,5,5,5-heptamethyl trisiloxane instead of 1,1,3,3,3-pentamethyl disiloxane and 3-butenol instead of allylalcohol. After distillation at 78° C./0.1×102 Pa, 83% of a clear liquid product was obtained.

후처리

  1. customThe reaction of Example 2a
  2. distillationAfter distillation at 78° C./0.1×102 Pa

출처 및 근거

ORD 기록
ord-fbdc354633e04642b7bebafc575bbe3b
출처 데이터셋
uspto-grants-2002_07
특허 번호
US06416746B1

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