Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzenamine, 4-(4-fluorophenoxy)- → [4-(4-Fluoro-phenoxy)-phenyl]-(2-methyl-6-nitro-phenyl)-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzenamine, 4-(4-fluorophenoxy)- | HCID 147633 | — |
| 반응물 | 2-Fluoro-1-methyl-3-nitrobenzene | HCID 13470957 | — |
| 반응물 | Potassium tert-butoxide | HCID 23665647 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | [4-(4-Fluoro-phenoxy)-phenyl]-(2-methyl-6-nitro-phenyl)-amine | HCID 68837567 | — |
반응 단계
The product (790 mg) is obtained according to the method of stage 1 of Example 4, by using 900 μL of 2-fluoro-3-methyl-nitrobenzene and 2.6 g of 4-(4-fluoro-phenoxy)-phenylamine obtained in stage 2 of Example 5 in the presence of 2.36 g of potassium tert-butanolate in 80 mL of DMSO.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08207373B2 |
| 출처 데이터셋 | uspto-grants-2012_06 |
| ORD ID | ord-23473f25389845a294d96dba157a51d1 |
| 출처 메모 | uspto-grants-2012_06 |