2,2,2-Trichloroethanimidamide → HCID 178516502, 화합물

HRID 223131

반응식

HRID 223131 반응식
[Cl:1][C:2]([Cl:7])([Cl:6])[C:3]([NH2:5])=[NH:4].[C:8]([O-])(=O)[CH2:9][C:10](C)=[O:11]>>[OH:11][C:10]1[CH:9]=[CH:8][N:5]=[C:3]([C:2]([Cl:7])([Cl:6])[Cl:1])[N:4]=1

참가 물질

3

반응물 2

HCID 356082,2,2-TrichloroethanimidamideHCID 6971017Acetoacetate

생성물 1

HCID 178516502HCID 178516502, 화합물

실험 절차

The carboxylic ester compounds of the present invention may be prepared by reacting trichloroacetamidine with a selected acetoacetate to form the corresponding 4-hydroxy-2-trichloromethylpyrimidine, which is then reacted with a selected carboxylic acid chloride. These general reactions are illustrated below in equations (A) and (B). In equation (A), trichloroacetamidine is reacted with ethyl 2-chloroacetoacetate to form 5-chloro-4-hydroxy-6-methyl-2-trichloromethyl-pyrimidine. In equation (B), the 5-chloro-4-hydroxy-6-methyl-2-trichloromethylpyrimidine is reacted with trichloroacetyl chloride to form 5-chloro-6-methyl-4-trichloroacetoxy-2-trichloromethylpyrimidine. ##STR3##

출처 및 근거

ORD 기록
ord-f5ee539350084581ab50b6a0008f2c84
출처 데이터셋
uspto-grants-1982_10
특허 번호
US04352806

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