Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acenaphthene → Acenaphthylene, dodecahydro-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acenaphthene | HCID 6734 | — |
| 촉매 | Rhodium | HCID 23948 | — |
| 생성물 | Acenaphthylene, dodecahydro- | HCID 102215 | 100% |
반응 단계
Acenaphthene was hydrogenated by the same procedure as in Example 4 except that the catalyst was replaced by a 5% Rh/C catalyst and reaction was effected at 150° C. for 30 minutes. Perhydroacenaphthene was produced in a yield of 100%, containing 1.1% of No. 1 isomer, 3.6% of No. 2 isomer, and 4.4% of No. 3 isomer, indicating a selectivity of No. 4 isomer of 90.9%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04783565 |
| 출처 데이터셋 | uspto-grants-1988_11 |
| ORD ID | ord-be6d29ca0ef3479797b3f28ae27053c0 |
| 출처 메모 | uspto-grants-1988_11 |