Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acenaphthene → Acenaphthylene, dodecahydro-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acenaphthene | HCID 6734 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | Acenaphthylene, dodecahydro- | HCID 102215 | 99.6% |
반응 단계
Acenaphthene was hydrogenated by the same procedure as in Example 1 except that the catalyst was replaced by a 5% Pd/C catalyst and reaction was effected at 160° C. for 6 hours. No substantial change was observed in the distribution of reaction products at the end of 4 hour reaction. Perhydroacenaphthene was finally obtained in a yield of 99.6%. The yields of Nos. 1 to 4 isomers were 33.5%, 11.8%, 24.5%, and 29.7%, respectively.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04783565 |
| 출처 데이터셋 | uspto-grants-1988_11 |
| ORD ID | ord-2fa212b42f7747d288d4f74fe660711c |
| 출처 메모 | uspto-grants-1988_11 |