Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 19927721, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 1-(3-(Trifluoromethyl)phenyl)piperazine | HCID 4296 | — |
| 반응물 | 6-methoxy-7-(oxiranylmethoxy)-2H-1-benzopyran-2-one | HCID 19927717 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | HCID 19927721 | HCID 19927721 | 80% |
반응 단계
Method C (1.5 d at 45° C.); starting materials: 6-methoxy-7-(oxiranylmethoxy)-2H-1-benzopyran-2-one (example 86) and 1-(3-trifluoromethylphenyl)piperazine; yield 80%; fusion point 133°-135° C. (from methanol). Hydrochloride: method F; yield 83%; fusion point 125°-128° C. (decomposes; from isopropanol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05428038 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-6057111434ac468bbdef2a80a5866e2e |
| 출처 메모 | uspto-grants-1995_06 |