2-Methoxyethanol → 3-(Methanesulfinyl)-6-phenyl[1,2,4]triazolo[3,4-a]phthalazine

HRID 2232234노트

반응식

CO[C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:18]3[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=3)[C:12]3=[N:19][N:20]=[C:21]([S:22][CH3:23])[N:11]3[N:10]=2)=[CH:5][CH:4]=1.C[O:25]CCO>>[CH3:23][S:22]([C:21]1[N:11]2[N:10]=[C:9]([C:6]3[CH:7]=[CH:8][CH:3]=[CH:4][CH:5]=3)[C:18]3[C:13]([C:12]2=[N:19][N:20]=1)=[CH:14][CH:15]=[CH:16][CH:17]=3)=[O:25]

참가 물질

반응물 2

HCID 80192-Methoxyethanol

HCID 21283334HCID 21283334, 화합물

생성물 1

HCID 30712493-(Methanesulfinyl)-6-phenyl[1,2,4]triazolo[3,4-a]phthalazine

실험 절차

This compound is obtained by following the procedure of the foregoing example but substituting 6-phenyl-3-methylthio-1,2,4-triazolo[3,4-a]phthalazine for 6-(4-methoxyphenyl)-3-methylthio-1,2,4-triazolo[3,4-a]phthalazine. M.p. 215°-217° C. (Methylcellosolve®).

후처리

customThis compound is obtained

출처 및 근거

ORD 기록: ord-6a4eb99bf47c4b53943d1e6d2bfe6aff
출처 데이터셋: uspto-grants-1988_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04788186

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