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Water → 2-(4-Fluorophenyl)-8-vinylimidazo[1,2-a]pyrazine

HRID 2233079
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HRID 2233079 반응식
Cl[C:2]1[C:3]2[N:4]([CH:8]=[C:9]([C:11]3[CH:16]=[CH:15][C:14]([F:17])=[CH:13][CH:12]=3)[N:10]=2)[CH:5]=[CH:6][N:7]=1.O.C(=O)([O-])[O-].[Na+].[Na+].F[B-](F)(F)F.[C:30](P(C(C)(C)C)C(C)(C)C)(C)(C)[CH3:31]>O1CCOCC1.C1C=CC(/C=C/C(/C=C/C2C=CC=CC=2)=O)=CC=1.C1C=CC(/C=C/C(/C=C/C2C=CC=CC=2)=O)=CC=1.C1C=CC(/C=C/C(/C=C/C2C=CC=CC=2)=O)=CC=1.[Pd].[Pd]>[F:17][C:14]1[CH:15]=[CH:16][C:11]([C:9]2[N:10]=[C:3]3[C:2]([CH:30]=[CH2:31])=[N:7][CH:6]=[CH:5][N:4]3[CH:8]=2)=[CH:12][CH:13]=1
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7

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HCID 962WaterHCID 10340Sodium CarbonateHCID 44558591Tri-t-butylphosphine fluoroborateHCID 574387418-Chloro-2-(4-fluorophenyl)imidazo[1,2-A]pyrazine

생성물 1

HCID 574387402-(4-Fluorophenyl)-8-vinylimidazo[1,2-a]pyrazine수율 642.6%

시약·촉매·용매 2

HCID 9811564
Bis(dibenzylideneacetone)palladium
촉매
HCID 312751,4-Dioxane용매

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온도
95 °C

실험 절차

To a mixture of 8-chloro-2-(4-fluorophenyl)-imidazo[1,2-a]pyrazine (Example #6, Step A, 3.96 g, 16 mmol) in dioxane (80 mL) was added water (15.4 mL), sodium carbonate (EM Science, 5.08 g, 48 mmol), tri-t-butylphosphine tetrafluoroborate (Strem, 0.46 g, 1.6 mmol), and tris(dibenzylideneacetone)dipalladium(0) (0.73 g, 0.8 mmol). The reaction was degassed with nitrogen and then vinylboronic acid pinacolester (5.44 mL, 32 mmol) was added. The mixture was heated to about 95° C. for about 16 h. The reaction was cooled, EtOAc was added (250 mL), and the mixture was washed with water. The organic layer was dried over sodium sulfate, filtered, and evaporated. The residue was purified by FCC (33%-50% EtOAc/heptane). The residue was triturated with heptane and filtered to yield the title compound as a brown solid (2.46 g, 62%): LC/MS (Table 1, Method b) Rt=2.74 min; MS m/z: 240.3 (M+H)+.

후처리

  1. customThe reaction was degassed with nitrogen
  2. additionvinylboronic acid pinacolester (5.44 mL, 32 mmol) was added
  3. temperatureThe reaction was cooled
  4. additionEtOAc was added (250 mL)
  5. washthe mixture was washed with water
  6. dry with materialThe organic layer was dried over sodium sulfate
  7. filtrationfiltered
  8. customevaporated
  9. customThe residue was purified by FCC (33%-50% EtOAc/heptane)
  10. customThe residue was triturated with heptane
  11. filtrationfiltered

출처 및 근거

ORD 기록
ord-c81084fa5c8e49cd97f9962520398057
출처 데이터셋
uspto-grants-2010_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07709468B2

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