Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-Ethyl-2-n-butyl-11-phenyl-11-amino-undeca-4,8-dienal-oxime
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 반응물 | 3-Ethyl-3-n-butyl-12-phenyl-1-aza-1,5,9-cyclododecatriene | HCID 54523241 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Ethyl-2-n-butyl-11-phenyl-11-amino-undeca-4,8-dienal-oxime | HCID 73678919 | 100% |
반응 단계
The procedure described in Example 1(b) is repeated, except that 283.4 g (0.875 mol) of 3-n-butyl-3-ethyl-12-phenyl-1-aza-1,5,9-cyclododecatriene, 60.8 g (0.87 mol) of hydroxylamine hydrochloride, 50 ml of concentrated hydrochloric acid and 250 ml of water are used. Working up yields 310 g (0.87 mol) of 2-n-butyl-2-ethyl-11-phenyl-11-amino-undeca-4,8-dienal oxime; yield 99.5% of theory.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04355177 |
| 출처 데이터셋 | uspto-grants-1982_10 |
| ORD ID | ord-811b847bcc4049f289519692750ea915 |
| 출처 메모 | uspto-grants-1982_10 |