Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2,2-Dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal semicarbazone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Semicarbazide hydrochloride | HCID 11236 | — |
| 반응물 | 3,3-Dimethyl-12-isopropyl-1-aza-1,5,9-cyclododecatriene | HCID 557512 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2,2-Dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal semicarbazone | HCID 54254998 | 86% |
반응 단계
The procedure described in Example 1(b) is repeated, except that 23.3 g (0.1 mol) of 3,3-dimethyl-12-isopropyl-1-aza-1,5,9-cyclododecatriene, 20 g of 37% hydrochloric acid, 20 ml of water and 11.15 g (0.1 mol) of semicarbazide hydrochloride are used. Working up yields 26.5 g (0.086 mol) of 2,2-dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal semicarbazone; yield 86% of theory.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04355177 |
| 출처 데이터셋 | uspto-grants-1982_10 |
| ORD ID | ord-9aa670777b5f407bba7fb02256f2d00a |
| 출처 메모 | uspto-grants-1982_10 |