참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 4-Chloro-3-hydroxybenzoic acid | HCID 141872 | — |
| 생성물 | 4-Chloro-3-hydroxybenzoyl chloride | HCID 75464818 | — |
반응 단계
An amount of 1 g (5.57 mmol) of 4-chloro-3-hydroxy benzoic acid is added 10 ml (115.8 mmol) of oxalyl chloride and refluxed at 60° C. till the solid had gone into solution. After cooling, the mixture is evaporated to dryness to give 4-chloro-3-hydroxy-benzoyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07713994B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_05 |
|---|
| ORD ID | ord-16e6a048a2ed40ebae9f8496b1802c19 |
|---|
| 출처 메모 | uspto-grants-2010_05 |
|---|
