tert-Butyl 2-bromobutanoate → HCID 11474075, 화합물

HRID 2240909노트

반응식

HRID 2240909 반응식
[F:1][C:2]([F:16])([F:15])[CH2:3][NH:4][C:5]1[CH:6]=[C:7]([C:13]#[N:14])[C:8]([C:11]#[N:12])=[CH:9][CH:10]=1.Br[CH:18]([CH2:26][CH3:27])[C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20]>>[C:13]([C:7]1[CH:6]=[C:5]([N:4]([CH2:3][C:2]([F:15])([F:16])[F:1])[CH:18]([CH2:26][CH3:27])[C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20])[CH:10]=[CH:9][C:8]=1[C:11]#[N:12])#[N:14]

참가 물질

3

반응물 2

HCID 13124118tert-Butyl 2-bromobutanoateHCID 576337284-[(2,2,2-Trifluoroethyl)amino]-1,2-benzenedicarbonitrile

생성물 1

HCID 11474075HCID 11474075, 화합물

실험 절차

Synthesized in a manner similar to example 1B using 4-[(2,2,2-trifluoroethyl)amino]-1,2-benzenedicarbonitrile and tert-butyl 2-bromobutanoate: MS (ES) m/z 368 (M+1).

후처리

  1. customSynthesized in a manner similar to example 1B

출처 및 근거

ORD 기록
ord-40287081a9844072b354ef0a5ae5e43d
출처 데이터셋
uspto-grants-2010_05
특허 번호
US07723385B2

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