Thionyl Chloride → 1-(Chloromethyl)-4-(octyloxy)benzene

HRID 2241856

반응식

HRID 2241856 반응식
[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][C:7]([CH2:8][Cl:9])=[CH:6][CH:5]=1)[CH3:2].S(Cl)(Cl)=O.[CH2:16](OC1C=CC(CO)=CC=1)[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21]CC>C(Cl)Cl>[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][C:7]([CH2:8][Cl:9])=[CH:6][CH:5]=1)[CH2:2][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

참가 물질

5

반응물 3

HCID 24386Thionyl ChlorideHCID 144261p-Octyloxybenzyl alcoholHCID 20639711-(Chloromethyl)-4-Ethoxybenzene

생성물 1

HCID 146742861-(Chloromethyl)-4-(octyloxy)benzene

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

This compound was synthesized following the same general procedure as that for the preparation of 4-ethoxybenzyl chloride; thionyl chloride (6.36 g, 53.4 mmol), 4-octyloxybenzyl alcohol (12.4 g, 52.5 mmol), CH2Cl2 (150 mL).

후처리

  1. customThis compound was synthesized

출처 및 근거

ORD 기록
ord-2efc181edf924ec9a8b065fcbc3c2897
출처 데이터셋
uspto-grants-2010_03
특허 번호
US07671033B2

연결된 노트

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