Thionyl Chloride → 4-Decyloxybenzyl Chloride

HRID 2241858노트

반응식

HRID 2241858 반응식
[CH2:1]([O:13][C:14]1[CH:21]=[CH:20][C:17]([CH2:18][Cl:19])=[CH:16][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10]CC.S(Cl)(Cl)=O.C(OC1C=CC(CO)=CC=1)CCCCCCCCC>C(Cl)Cl>[CH2:1]([O:13][C:14]1[CH:21]=[CH:20][C:17]([CH2:18][Cl:19])=[CH:16][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

참가 물질

5

반응물 3

HCID 24386Thionyl ChlorideHCID 100867551-(Chloromethyl)-4-(dodecyloxy)benzeneHCID 130796524-Decyloxybenzyl alcohol

생성물 1

HCID 201490124-Decyloxybenzyl Chloride

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

Was synthesized following the same general procedure as that for the preparation of 4-dodecyloxybenzyl chloride; thionyl chloride (5.00 g, 42.4 mmol), 4-decyloxybenzyl alcohol (10.2 g, 38.6 mmol), CH2Cl2 (100 mL). 9.87 g (90%) white solid which decomposes upon melting.

후처리

  1. customWas synthesized

출처 및 근거

ORD 기록
ord-a033880df3c848cfbf8807a3cf38d580
출처 데이터셋
uspto-grants-2010_03
특허 번호
US07671033B2

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